夜雨聆风
科研小记 | XRD标准卡片 PDF#01-074-0505和PDF# 00-038-0715
PDF#01-074-0505(RDB)(作废相):质标=定胞(I);d=计算值;I=计算值
Cesium Zirconium Chloride
Cs2 Zr Cl6
射线=CuKa1 波长=1.5406 滤波法=
校准= 2θ=14.731-89.833 I/Ic(K值)=6.1
文献: Engel, G.
Z. Kristallogr., Kristallgeom., Kristallphys., Kristallchem., v90 p341(1935)
立方晶系-(未知),Fm-3m(225) Z=4
晶胞: 10.407×10.407×10.407 <90.0×90.0x90.0> P.S=cF36.00
密度(计算)=3.357 密度(测量)= 分子量=569.75 体积=1127.14 F(30)=999.9(0,30/0)
文献: 出处同上
强峰线: 3.68/X 2.60/7 3.00/7 6.01/4 1.84/4 2.12/4 1.57/2 1.65/2
ANX: AB2X6.
Delete duplicate: Delete: ICSD 2008/1 version removed this collection code.
See PDF 01-074-1001 SK 1/09.
ICSD Collection Code: 26135.
Test from external database: No R value given.
At least one TF missing.
Minor Warning: No R value given in the paper.
Wyckoff Sequence: e b a (FM3-M).
2θ d(埃) I(f) ( h k l) θ 1/(2d) 2π/d n^2
14.731 6.0085 44.5 ( 1 1 1) 7.366 0.0832 1.0457 3
17.026 5.2035 12.6 ( 2 0 0) 8.513 0.0961 1.2075 4
24.169 3.6794 100.0 ( 2 2 0) 12.084 0.1359 1.7077 8
28.421 3.1378 12.1 ( 3 1 1) 14.211 0.1593 2.0024 11
29.713 3.0042 72.9 ( 2 2 2) 14.857 0.1664 2.0914 12
34.443 2.6018 73.9 ( 4 0 0) 17.222 0.1922 2.4150 16
37.644 2.3875 2.4 ( 3 3 1) 18.822 0.2094 2.6317 19
38.661 2.3271 6.6 ( 4 2 0) 19.330 0.2149 2.7000 20
42.521 2.1243 36.5 ( 4 2 2) 21.260 0.2354 2.9577 24
45.238 2.0028 7.4 ( 5 1 1) 22.619 0.2496 3.1372 27
49.506 1.8397 41.4 ( 4 4 0) 24.753 0.2718 3.4153 32
51.939 1.7591 5.8 ( 5 3 1) 25.969 0.2842 3.5718 35
52.732 1.7345 3.2 ( 4 4 2) 26.366 0.2883 3.6225 36
55.825 1.6455 15.7 ( 6 2 0) 27.913 0.3039 3.8184 40
58.072 1.5871 1.2 ( 5 3 3) 29.036 0.3150 3.9590 43
58.809 1.5689 18.8 ( 6 2 2) 29.405 0.3187 4.0048 44
61.702 1.5021 11.9 ( 4 4 4) 30.851 0.3329 4.1829 48
63.820 1.4573 3.2 ( 7 1 1) 31.910 0.3431 4.3116 51
64.518 1.4432 1.1 ( 6 4 0) 32.259 0.3465 4.3537 52
67.269 1.3907 15.3 ( 6 4 2) 33.635 0.3595 4.5180 56
69.296 1.3549 1.7 ( 7 3 1) 34.648 0.3690 4.6374 59
72.618 1.3009 4.7 ( 8 0 0) 36.309 0.3844 4.8300 64
74.581 1.2714 0.1 ( 7 3 3) 37.290 0.3933 4.9419 67
75.231 1.2620 1.5 ( 8 2 0) 37.616 0.3962 4.9786 68
77.813 1.2265 6.2 ( 8 2 2) 38.907 0.4077 5.1229 72
79.734 1.2017 1.3 ( 7 5 1) 39.867 0.4161 5.2286 75
80.372 1.1938 5.6 ( 6 6 2) 40.186 0.4188 5.2634 76
82.909 1.1635 11.7 ( 8 4 0) 41.455 0.4297 5.4001 80
84.804 1.1423 1.2 ( 9 1 1) 42.402 0.4377 5.5004 83
85.434 1.1355 1.2 ( 8 4 2) 42.717 0.4403 5.5334 84
87.949 1.1094 3.1 ( 6 6 4) 43.975 0.4507 5.6636 88
89.833 1.0910 1.1 ( 9 3 1) 44.917 0.4583 5.7594 91
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PDF#00-038-0715(RDB):质标=空白(B);d=(未知);I=(未知)
Jamborite, syn(Nickel Hydroxide Hydrate)
Ni ( O H )2 ·0.75 H2 O
射线=CuKa1 波长=1.5406 滤波法=
校准= 2θ=11.350-61.255 I/Ic(K值)=
文献: Braconnier, J., Delmas, C., Fouassier, C., Figlarz, M., Beaudouin, B., Hagenmuller, P.
Rev. Chim. Miner., v21 p496(1984)
菱面晶系-(未知),R Z=
晶胞: 3.08×3.08×23.41 <90.0×90.0x120.0> P.S=hR?(á*)
密度(计算)= 密度(测量)= 分子量=106.23 体积=192.32 F(8)=7(0.076,15/0)
文献: 出处同上
强峰线: 7.79/X 3.91/7 2.60/5 2.32/5 1.54/5 2.68/5 1.51/2 1.97/2
General Comments: $GA* indicates the difference in structure and texture.
2θ d(埃) I(f) ( h k l) θ 1/(2d) 2π/d n^2
11.350 7.7900 100.0 ( 0 0 3) 5.675 0.0642 0.8066
22.736 3.9080 70.0 ( 0 0 6) 11.368 0.1279 1.6078
33.459 2.6760 50.0 ( 1 0 1) 16.729 0.1868 2.3480
34.412 2.6040 50.0 ( 0 1 2) 17.206 0.1920 2.4129
38.766 2.3210 50.0 ( 0 1 5) 19.383 0.2154 2.7071
45.986 1.9720 20.0 ( 0 1 8) 22.993 0.2535 3.1862
59.982 1.5410 50.0 ( 1 1 0) 29.991 0.3245 4.0773
61.255 1.5120 20.0 ( 1 1 3) 30.627 0.3307 4.1555
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