夜雨聆风
科研小记 | XRD标准卡片 PDF#00-025-0823和PDF# 00-010-0340
PDF#00-025-0823(RDB):质标=空白(B);d=(未知);I=胶片/目测
Sodium Cobalt Silicate
Na2 Co Si O4 Dark blue
射线=CrKa1 波长=2.2897 滤波法=V
校准= 2θ=20.639-48.376 I/Ic(K值)=
文献: Wintenberger, Lab. Diffract. Neutronique Ceng., Grenoble.
Private Communication(1971)
单斜晶系-粉末衍射,Pn(7) Z=2
晶胞: 7.07×5.46×5.22 <90.0×90.0x90.0> P.S=mP16.00
密度(计算)=3.247 密度(测量)= 分子量=197 体积=201.50 F(9)=4.5(0.087,23/0)
文献: Wintenberger.
C. R. Seances Acad. Sci., Ser. B, v271 p669(1970)
强峰线: 2.58/X 2.61/8 2.95/7 4.30/6 2.73/6 4.20/6 2.42/2 1.88/1
Color: Dark blue.
Unit Cell Data Source: Powder Diffraction.
2θ d(埃) I(f) ( h k l) θ 1/(2d) 2π/d n^2
20.639 4.3000 60.0 ( 1 1 0) 10.320 0.1163 1.4612
21.136 4.2000 60.0 (-1 0 1) 10.568 0.1190 1.4960
30.273 2.9500 70.0 ( 2 1 0) 15.136 0.1695 2.1299
32.778 2.7300 60.0 ( 0 2 0) 16.389 0.1832 2.3015
34.331 2.6100 80.0 ( 0 0 2) 17.165 0.1916 2.4074
34.743 2.5800 100.0 (-2 1 1) 17.371 0.1938 2.4353
37.121 2.4200 20.0 ( 0 2 1) 18.560 0.2066 2.5964
46.284 1.9600 10.0 (-2 1 2) 23.142 0.2551 3.2057
48.376 1.8800 10.0 ( 0 2 2) 24.188 0.2660 3.3421
请在微信客户端打开
附图：
PDF#00-010-0340(RDB):质标=定胞(I);d=其它/未知(340mm);I=衍射仪
Chromium Sulfide
Cr2 S3
射线=MoKa1 波长=0.7093 滤波法=Zr
校准= 2θ=15.956-138.768 I/Ic(K值)=
文献: Jellinek.
Acta Crystallogr., v10 p620(1957)
菱面晶系-粉末衍射,R-3(148) Z=6
晶胞: 5.939×5.939×16.65 <90.0×90.0x120.0> P.S=hR10.00
密度(计算)=3.921 密度(测量)= 分子量=200.17 体积=508.59 F(30)=16.8(0.029,61/0)
文献: 出处同上
强峰线: 2.02/X 2.61/8 1.71/5 1.04/3 1.57/3 1.31/2 1.08/2 2.96/2
Additional Patterns: See PDF 01-072-1224.
Additional Diffraction Lines: Plus 13 additional reflections to 0.689.
Unit Cell: Rhombohedral cell: a=6.524, $GA=54.15?.
Unit Cell Data Source: Powder Diffraction.
2θ d(埃) I(f) ( h k l) θ 1/(2d) 2π/d n^2
15.956 5.5500 16.0 ( 0 0 3) 7.978 0.0901 1.1321
18.052 4.9100 10.0 ( 1 0 1) 9.026 0.1018 1.2797
20.305 4.3700 8.0 ( 0 1 2) 10.153 0.1144 1.4378
27.594 3.2300 6.0 ( 1 0 4) 13.797 0.1548 1.9453
30.168 2.9600 16.0 ( 1 1 0) 15.084 0.1689 2.1227
32.137 2.7830 6.0 ( 0 0 6) 16.068 0.1797 2.2577
34.290 2.6130 80.0 ( 1 1 3) 17.145 0.1914 2.4046
35.510 2.5260 2.0 ( 0 2 1) 17.755 0.1979 2.4874
36.542 2.4570 2.0 ( 2 0 2) 18.271 0.2035 2.5573
41.384 2.1800 4.0 ( 0 2 4) 20.692 0.2294 2.8822
44.739 2.0240 100.0 ( 1 1 6) 22.370 0.2470 3.1043
47.150 1.9260 4.0 ( 0 1 8) 23.575 0.2596 3.2623
47.835 1.9000 2.0 ( 1 2 2) 23.917 0.2632 3.3069
49.240 1.8490 4.0 ( 0 0 9) 24.620 0.2704 3.3982
51.942 1.7590 4.0 ( 2 1 4) 25.971 0.2843 3.5720
52.261 1.7490 2.0 ( 0 2 7) 26.131 0.2859 3.5924
53.446 1.7130 50.0 ( 3 0 0) 26.723 0.2919 3.6679
54.652 1.6780 4.0 ( 1 2 5) 27.326 0.2980 3.7444
56.178 1.6360 8.0 ( 3 0 3) 28.089 0.3056 3.8406
58.806 1.5690 25.0 ( 1 1 9) 29.403 0.3187 4.0046
62.539 1.4840 4.0 ( 2 2 0) 31.270 0.3369 4.2340
65.033 1.4330 10.0 ( 2 2 3) 32.516 0.3489 4.3846
65.547 1.4230 4.0 ( 1 3 1) 32.773 0.3514 4.4155
67.417 1.3880 12.0 (0,0,12) 33.708 0.3602 4.5268
69.760 1.3470 2.0 ( 1 3 4) 34.880 0.3712 4.6646
72.159 1.3080 20.0 ( 2 2 6) 36.080 0.3823 4.8037
75.514 1.2580 8.0 ( 3 0 9) 37.757 0.3975 4.9946
83.394 1.1580 8.0 ( 2 2 9) 41.697 0.4318 5.4259
86.713 1.1220 4.0 ( 4 1 0) 43.357 0.4456 5.6000
87.789 1.1110 2.0 (0,0,15) 43.895 0.4500 5.6554
88.999 1.0990 12.0 ( 4 1 3) 44.500 0.4550 5.7172
91.106 1.0790 20.0 (2,0,14) 45.553 0.4634 5.8232
95.577 1.0400 25.0 (1,1,15) 47.788 0.4808 6.0415
102.313 0.9890 8.0 ( 3 3 0) 51.157 0.5056 6.3531
106.879 0.9590 8.0 ( 4 1 9) 53.439 0.5214 6.5518
120.103 0.8890 4.0 (2,2,15) 60.051 0.5624 7.0677
121.468 0.8830 6.0 (1,1,18) 60.734 0.5663 7.1157
128.009 0.8570 4.0 ( 6 0 0) 64.004 0.5834 7.3316
138.768 0.8230 2.0 ( 5 2 0) 69.384 0.6075 7.6345
附图：
感谢你读到这里
七七想与你分享每一个前进的脚印🌼