夜雨聆风
科研小记 | XRD标准卡片 PDF#00-044-0003和PDF#00-007-0235
PDF#00-044-0003(RDB):质标=星印(S);d=衍射仪;I=衍射仪
Aluminum Silicate
Al2 O3 ·54 Si O2
射线=CuKa1 波长=1.5406 滤波法=
校准= 2θ=7.972-47.327 I/Ic(K值)=
文献: Alvarez, A., Viturro, H., Bonetto, R.
Private Communication
正交晶系-(未知),Pnma(62) Z=
晶胞: 20.104×19.897×13.395 <90.0×90.0x90.0> P.S=oP?
密度(计算)= 密度(测量)= 分子量=3346.51 体积=5358.12 F(30)=19.8(0.022,69/0)
文献: 出处同上
强峰线: 11.08/X 9.91/7 10.02/6 3.81/6 3.85/5 3.71/3 3.75/2 9.69/2
Additional Patterns: See PDF 01-084-0385.
Sample Source or Locality: Sample prepared at the Engineering Laboratory, Universidad Complutense de Madrid.
2θ d(埃) I(f) ( h k l) θ 1/(2d) 2π/d n^2
7.972 11.0814 100.0 ( 1 0 1) 3.986 0.0451 0.5670
8.818 10.0201 64.0 ( 2 0 0) 4.409 0.0499 0.6271
8.917 9.9091 70.0 ( 0 2 0) 4.458 0.0505 0.6341
9.123 9.6858 17.0 ( 1 1 1) 4.561 0.0516 0.6487
9.878 8.9471 2.0 ( 2 1 0) 4.939 0.0559 0.7023
11.033 8.0129 1.0 ( 2 0 1) 5.516 0.0624 0.7841
11.945 7.4031 2.0 ( 1 2 1) 5.972 0.0675 0.8487
12.540 7.0531 1.0 ( 2 2 0) 6.270 0.0709 0.8908
13.243 6.6803 4.0 ( 0 0 2) 6.621 0.0748 0.9406
13.953 6.3419 8.0 ( 1 0 2) 6.976 0.0788 0.9907
14.787 5.9860 11.0 ( 3 0 1) 7.393 0.0835 1.0496
14.930 5.9290 5.0 ( 0 3 1) 7.465 0.0843 1.0597
15.558 5.6911 8.0 ( 1 3 1) 7.779 0.0879 1.1040
15.920 5.5625 7.0 ( 2 0 2) 7.960 0.0899 1.1296
16.557 5.3499 2.0 ( 1 2 2) 8.278 0.0935 1.1745
17.275 5.1291 2.0 ( 3 2 1) 8.637 0.0975 1.2250
17.650 5.0210 4.0 ( 4 0 0) 8.825 0.0996 1.2514
17.830 4.9707 8.0 ( 0 4 0) 8.915 0.1006 1.2641
19.250 4.6071 3.0 ( 3 1 2) 9.625 0.1085 1.3638
19.925 4.4525 1.0 ( 2 4 0) 9.962 0.1123 1.4112
20.368 4.3567 4.0 ( 1 0 3) 10.184 0.1148 1.4422
20.870 4.2530 7.0 ( 1 1 3) 10.435 0.1176 1.4774
21.767 4.0797 1.0 ( 2 0 3) 10.883 0.1226 1.5401
22.175 4.0056 3.0 ( 4 3 0) 11.087 0.1248 1.5686
23.080 3.8505 48.0 ( 3 3 2) 11.540 0.1299 1.6318
23.320 3.8114 59.0 ( 0 5 1) 11.660 0.1312 1.6485
23.720 3.7480 17.0 ( 1 5 1) 11.860 0.1334 1.6764
23.950 3.7126 29.0 ( 3 0 3) 11.975 0.1347 1.6924
24.415 3.6429 16.0 ( 1 3 3) 12.207 0.1373 1.7248
24.778 3.5903 1.0 ( 5 2 1) 12.389 0.1393 1.7500
25.570 3.4809 2.0 ( 3 2 3) 12.785 0.1436 1.8050
25.897 3.4377 4.0 ( 4 3 2) 12.948 0.1454 1.8277
26.215 3.3967 2.0 ( 5 1 2) 13.107 0.1472 1.8498
26.407 3.3724 1.0 ( 1 5 2) 13.203 0.1483 1.8631
26.575 3.3515 3.0 ( 6 0 0) 13.287 0.1492 1.8747
26.868 3.3156 7.0 ( 0 6 0) 13.434 0.1508 1.8950
26.967 3.3037 2.0 ( 6 1 0) 13.483 0.1513 1.9019
27.510 3.2397 1.0 ( 3 3 3) 13.755 0.1543 1.9394
28.052 3.1783 1.0 ( 1 6 1) 14.026 0.1573 1.9769
29.275 3.0483 4.0 ( 3 5 2) 14.637 0.1640 2.0612
29.862 2.9897 4.0 ( 6 3 0) 14.931 0.1672 2.1016
30.065 2.9699 3.0 ( 0 5 3) 15.032 0.1684 2.1156
30.365 2.9413 2.0 ( 1 6 2) 15.182 0.1700 2.1362
31.198 2.8646 1.0 ( 5 2 3) 15.599 0.1745 2.1934
32.740 2.7331 2.0 ( 2 7 0) 16.370 0.1829 2.2989
34.360 2.6079 2.0 ( 5 5 2) 17.180 0.1917 2.4093
34.641 2.5874 1.0 ( 6 2 3) 17.320 0.1932 2.4284
34.940 2.5659 1.0 ( 3 4 4) 17.470 0.1949 2.4487
35.675 2.5147 2.0 ( 8 0 0) 17.837 0.1988 2.4986
37.200 2.4150 2.0 ( 7 0 3) 18.600 0.2070 2.6017
37.508 2.3959 1.0 ( 3 5 4) 18.754 0.2087 2.6225
45.053 2.0107 5.0 (10,0,0) 22.526 0.2487 3.1250
45.530 1.9907 8.0 (0,10,0) 22.765 0.2512 3.1563
46.447 1.9535 1.0 ( 7 6 3) 23.223 0.2560 3.2164
47.327 1.9192 1.0 ( 8 6 2) 23.663 0.2605 3.2739
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PDF#00-007-0235(RDB):质标=星印(S);d=(未知);I=衍射仪
Lead Iodide
Pb I2 Orange
射线=CuKa1 波长=1.5405 滤波法=Ni
校准= 2θ=12.672-126.874 I/Ic(K值)=4.2
文献:
Natl. Bur. Stand. (U.S.), Circ. 539, v5 p34(1955)
六方晶系-粉末衍射,P-3m1(164) Z=1
晶胞: 4.557×4.557×6.979 <90.0×90.0x120.0> P.S=hP3.00
密度(计算)=6.099 密度(测量)= 分子量=461.01 体积=125.51 F(30)=51.6(0.0124,47/0)
文献:
强峰线: 3.44/X 2.61/6 2.28/5 6.98/3 1.90/2 2.01/2 2.17/1 1.72/1
Analysis: Spectroscopic analysis shows <0.01% Al, Bi, Fe, Si; <0.001% Ag, Ca, Cr, Cu, Mg.
Color: Orange.
Sample Preparation: Sample prepared at NBS from ”Pb C O3” and HI.
Temperature of Data Collection: Pattern taken at 298 K.
Unit Cell Data Source: Powder Diffraction.
2θ d(埃) I(f) ( h k l) θ 1/(2d) 2π/d n^2
12.672 6.9800 25.0 ( 0 0 1) 6.336 0.0716 0.9002
22.520 3.9450 6.0 ( 1 0 0) 11.260 0.1267 1.5927
25.509 3.4890 4.0 ( 0 0 2) 12.755 0.1433 1.8009
25.917 3.4350 100.0 ( 1 0 1) 12.959 0.1456 1.8292
34.277 2.6140 55.0 ( 1 0 2) 17.138 0.1913 2.4037
38.662 2.3270 6.0 ( 0 0 3) 19.331 0.2149 2.7001
39.528 2.2780 45.0 ( 1 1 0) 19.764 0.2195 2.7582
41.662 2.1661 14.0 ( 1 1 1) 20.831 0.2308 2.9007
45.182 2.0052 16.0 ( 1 0 3) 22.591 0.2494 3.1334
47.843 1.8997 18.0 ( 2 0 1) 23.921 0.2632 3.3075
52.394 1.7449 6.0 ( 0 0 4) 26.197 0.2865 3.6009
53.305 1.7172 14.0 ( 2 0 2) 26.652 0.2912 3.6590
56.494 1.6276 8.0 ( 1 1 3) 28.247 0.3072 3.8604
57.752 1.5951 2.0 ( 1 0 4) 28.876 0.3135 3.9391
61.603 1.5043 4.0 ( 2 0 3) 30.801 0.3324 4.1768
63.775 1.4582 12.0 ( 2 1 1) 31.887 0.3429 4.3089
67.572 1.3852 8.0 ( 1 1 4) 33.786 0.3610 4.5359
68.356 1.3712 10.0 ( 2 1 2) 34.178 0.3646 4.5823
71.665 1.3158 8.0 ( 1 0 5) 35.833 0.3800 4.7752
73.144 1.2928 2.0 ( 3 0 1) 36.572 0.3868 4.8601
75.684 1.2556 4.0 ( 2 1 3) 37.842 0.3982 5.0041
84.568 1.1449 2.0 ( 3 0 3) 42.284 0.4367 5.4880
85.072 1.1394 4.0 ( 2 0 5) 42.536 0.4388 5.5145
87.306 1.1159 2.0 ( 1 0 6) 43.653 0.4481 5.6306
90.879 1.0811 4.0 ( 3 1 1) 45.440 0.4625 5.8118
94.333 1.0504 4.0 ( 3 0 4) 47.167 0.4760 5.9817
95.070 1.0442 4.0 ( 3 1 2) 47.535 0.4788 6.0172
97.659 1.0233 2.0 ( 2 2 3) 48.830 0.4886 6.1401
98.214 1.0190 4.0 ( 2 1 5) 49.107 0.4907 6.1660
102.112 0.9904 2.0 ( 3 1 3) 51.056 0.5048 6.3441
104.093 0.9769 <1 ( 4 0 1) 52.046 0.5118 6.4318
107.676 0.9541 2.0 ( 2 2 4) 53.838 0.5241 6.5855
108.456 0.9494 2.0 ( 4 0 2) 54.228 0.5266 6.6181
112.339 0.9273 2.0 ( 3 1 4) 56.169 0.5392 6.7758
114.245 0.9172 2.0 ( 2 1 6) 57.123 0.5451 6.8504
118.203 0.8977 2.0 ( 3 2 1) 59.101 0.5570 6.9992
126.874 0.8612 2.0 ( 4 1 0) 63.437 0.5806 7.2959
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