夜雨聆风
PDF#00-016-0613(RDB):质标=定胞(I);d=Guinier;I=光密度议
Vermiculite-2M
Mgx ( Mg , Fe )3 ( Si , Al )4 O10 ( O H )2 ·4 H2 O Brown, green
射线=CuKa 波长=1.5418 滤波法=
校准= 2θ=6.219-61.707 I/Ic(K值)=
文献: Mukherjee.
Clay Miner. Bull., v5 p194(1963)
单斜晶系-粉末衍射,C2/c(15) Z=4
晶胞: 5.24x9.17x28.6 <90.0x94.6x90.0> P.S=mC136.00
密度(计算)=2.260 密度(测量)=2.28 分子量=475.63 体积=1369.83 F(30)=2.7(0.054,203/0)
文献: Shirozu, H., Bailey, S.
Am. Mineral., v51 p1124(1966)
强峰线: 14.20/X 1.53/7 4.57/6 2.57/5 2.62/5 2.53/5 2.37/4 2.38/4
Additional Patterns: To replace 00-010-0418 and validated by calculated pattern 00-034-0166.
See PDF 01-077-0022 and 01-076-0847.
Analysis: Analysis (wt.%): ''Si O2'' 34.92, ''Al2 O3'' 13.97, ''Fe2 O3'' 6.25, FeO 0.52, MgO 20.37, CaO 2.15, ''Na2 O'' 0.32, ''H2 O'' 21.00.
Color: Brown, green.
Sample Source or Locality: Specimen from Ajmer-Marwar, India (Indian Museum 8247).
Unit Cell Data Source: Powder Diffraction.
2θ d(埃) I(f) ( h k l) θ 1/(2d) 2π/d n^2
6.219 14.2000 100.0 ( 0 0 2) 3.110 0.0352 0.4425
12.387 7.1400 15.0 ( 0 0 4) 6.193 0.0700 0.8800
18.626 4.7600 10.0 ( 0 0 6) 9.313 0.1050 1.3200
19.408 4.5700 60.0 ( 0 2 0) 9.704 0.1094 1.3749
20.119 4.4100 10.0 (-1 1 2) 10.059 0.1134 1.4248
20.399 4.3500 10.0 ( 0 2 2) 10.200 0.1149 1.4444
20.885 4.2500 10.0 ( 1 1 2) 10.442 0.1176 1.4784
24.992 3.5600 25.0 ( 0 0 8) 12.496 0.1404 1.7649
31.362 2.8500 30.0 (0,0,10) 15.681 0.1754 2.2046
34.263 2.6150 50.0 (-1 3 2) 17.132 0.1912 2.4027
34.882 2.5700 50.0 (-1 3 3) 17.441 0.1946 2.4448
35.524 2.5250 45.0 (-2 0 4) 17.762 0.1980 2.4884
36.962 2.4300 5.0 (-1 3 5) 18.481 0.2058 2.5857
37.768 2.3800 35.0 (0,0,12) 18.884 0.2101 2.6400
38.017 2.3650 35.0 (-2 0 6) 19.008 0.2114 2.6567
39.764 2.2650 5.0 (-2 2 2) 19.882 0.2208 2.7740
40.991 2.2000 5.0 (-2 2 4) 20.496 0.2273 2.8560
41.584 2.1700 5.0 (-1,1,12) 20.792 0.2304 2.8955
43.472 2.0800 5.0 ( 1 3 8) 21.736 0.2404 3.0208
44.370 2.0400 10.0 (0,0,14) 22.185 0.2451 3.0800
45.068 2.0100 10.0 (-2,0,10) 22.534 0.2488 3.1260
45.912 1.9750 5.0 (-1,3,10) 22.956 0.2532 3.1814
50.079 1.8200 5.0 (1,3,11) 25.039 0.2747 3.4523
50.977 1.7900 5.0 ( 2 2 9) 25.489 0.2793 3.5102
53.045 1.7250 10.0 (-2 4 1) 26.522 0.2899 3.6424
53.379 1.7150 10.0 (-3 1 1) 26.689 0.2915 3.6637
54.059 1.6950 5.0 (-2 4 4) 27.030 0.2950 3.7069
55.115 1.6650 15.0 (-1 5 5) 27.558 0.3003 3.7737
59.897 1.5430 10.0 ( 1 5 8) 29.948 0.3240 4.0721
60.546 1.5280 70.0 ( 0 6 0) 30.273 0.3272 4.1120
61.165 1.5140 25.0 (1,3,15) 30.583 0.3303 4.1501
61.707 1.5020 15.0 ( 1 5 9) 30.854 0.3329 4.1832
附图：
PDF#00-037-1484(RDB):质标=星印(S);d=衍射仪;I=衍射仪
Baddeleyite, syn(Zirconium Oxide)
Zr O2 Colorless
射线=CuKa1 波长=1.5405982 滤波法=Graph
校准=内部(Ag FP) 2θ=17.419-78.866 I/Ic(K值)=2.6
文献: McMurdie, H., Morris, M., Evans, E., Paretzkin, B., Wong-Ng, W., Hubbard, C.
Powder Diffraction, v1 p275(1986)
单斜晶系-粉末衍射,P21/a(14) Z=4
晶胞: 5.3129x5.2125x5.1471 <90.0x99.218x90.0> P.S=mP12.00
密度(计算)=5.817 密度(测量)= 分子量=123.22 体积=140.70 F(30)=111.1(0.0073,37/0)
文献: (1) McCullough, J., Trueblood, K.
Acta Crystallogr., v12 p507(1959)
强峰线: 3.16/X 2.84/7 1.82/2 2.62/2 1.85/2 3.70/1 2.54/1 1.80/1
Additional Patterns: To replace 00-013-0307 and 00-036-0420 and validated by calculated pattern 00-024-1165.
See PDF 01-072-1669, 01-072-0597, 01-074-0815 and 01-078-0050.
Analysis: Spectrographic analysis showed that this sample contained less than 0.01% each of Al, Hf and Mg and between 0.1 and 0.01% each of Fe, Si and Ti.
Color: Colorless.
General Comments: Pattern reviewed by Holzer, J., McCarthy, G., North Dakota State Univ., Fargo, North Dakota, USA, ICDD Grant-in-Aid (1990).
Agrees well with experimental and calculated patterns.
Additional weak reflections (indicated by brackets) were observed.
Polymorphism/Phase Transition: There are a number of polymorphic forms of ''Zr O2'' stable at different temperatures and pressures.
Sample Source or Locality: Sample was obtained from Titanium Alloy Manufacturing Co.
(1990) and was heated to 1300° for 48 hours.
Structures: The structure of ''Zr O2'' (baddeleyite) was determined by McCullough and Trueblood (1) and confirmed by Smith and Newkirk (2).
Temperature of Data Collection: The mean temperature of the data collection was 298.5 K.
Unit Cell Data Source: Powder Diffraction.
2θ d(埃) I(f) ( h k l) θ 1/(2d) 2π/d n^2
17.419 5.0870 3.0 ( 0 0 1) 8.709 0.0983 1.2351
24.048 3.6977 14.0 ( 1 1 0) 12.024 0.1352 1.6992
24.441 3.6391 10.0 ( 0 1 1) 12.220 0.1374 1.7266
28.175 3.1647 100.0 (-1 1 1) 14.087 0.1580 1.9854
31.468 2.8406 68.0 ( 1 1 1) 15.734 0.1760 2.2119
34.160 2.6227 21.0 ( 2 0 0) 17.080 0.1906 2.3957
34.383 2.6062 11.0 ( 0 2 0) 17.191 0.1919 2.4109
35.309 2.5399 13.0 ( 0 0 2) 17.654 0.1969 2.4738
35.900 2.4995 2.0 (-2 0 1) 17.950 0.2000 2.5138
38.396 2.3425 1.0 (-2 1 0) 19.198 0.2134 2.6823
38.541 2.3340 4.0 ( 1 2 0) 19.270 0.2142 2.6920
39.411 2.2845 <1 ( 0 1 2) 19.705 0.2189 2.7504
39.990 2.2527 <1 (-2 1 1) 19.995 0.2220 2.7891
40.725 2.2138 12.0 (-1 1 2) 20.362 0.2259 2.8382
41.150 2.1919 5.0 ( 2 0 1) 20.575 0.2281 2.8666
41.374 2.1805 5.0 (-1 2 1) 20.687 0.2293 2.8815
44.826 2.0203 7.0 ( 2 1 1) 22.413 0.2475 3.1100
45.522 1.9910 6.0 (-2 0 2) 22.761 0.2511 3.1558
48.949 1.8593 2.0 (-2 1 2) 24.474 0.2689 3.3793
49.266 1.8481 18.0 ( 2 2 0) 24.633 0.2705 3.3998
50.116 1.8187 22.0 ( 0 2 2) 25.058 0.2749 3.4547
50.559 1.8038 13.0 (-2 2 1) 25.279 0.2772 3.4832
51.193 1.7830 5.0 (-1 2 2) 25.596 0.2804 3.5240
54.104 1.6937 11.0 ( 0 0 3) 27.052 0.2952 3.7097
54.680 1.6772 <1 ( 2 2 1) 27.340 0.2981 3.7462
55.270 1.6607 11.0 ( 1 2 2) 27.635 0.3011 3.7835
55.400 1.6571 11.0 ( 3 1 0) 27.700 0.3017 3.7916
55.570 1.6525 9.0 (-3 1 1) 27.785 0.3026 3.8023
55.883 1.6439 6.0 ( 0 3 1) 27.941 0.3041 3.8220
57.168 1.6100 7.0 (-1 1 3) 28.584 0.3106 3.9026
57.861 1.5924 4.0 (-1 3 1) 28.930 0.3140 3.9459
58.268 1.5822 3.0 (-2 2 2) 29.134 0.3160 3.9712
59.775 1.5459 8.0 ( 1 3 1) 29.887 0.3234 4.0645
60.055 1.5393 7.0 (-2 0 3) 30.027 0.3248 4.0818
61.366 1.5095 5.0 ( 3 1 1) 30.683 0.3312 4.1624
61.984 1.4960 5.0 (-3 1 2) 30.992 0.3342 4.2001
62.838 1.4777 8.0 ( 1 1 3) 31.419 0.3384 4.2521
64.079 1.4520 1.0 ( 3 2 0) 32.039 0.3444 4.3272
64.250 1.4486 2.0 ( 2 3 0) 32.125 0.3452 4.3375
64.965 1.4343 <1 ( 0 3 2) 32.483 0.3486 4.3806
65.383 1.4262 2.0 (-2 3 1) 32.692 0.3506 4.4057
65.700 1.4201 6.0 ( 0 2 3) 32.850 0.3521 4.4246
65.884 1.4165 4.0 (-1 3 2) 32.942 0.3530 4.4356
68.911 1.3615 1.0 ( 2 3 1) 34.456 0.3672 4.6149
69.620 1.3494 <1 ( 3 2 1) 34.810 0.3705 4.6564
70.190 1.3398 <1 (-3 2 2) 35.095 0.3732 4.6896
71.071 1.3253 2.0 (-2 2 3) 35.535 0.3773 4.7408
71.299 1.3217 4.0 (-4 0 1) 35.650 0.3783 4.7540
71.949 1.3113 1.0 ( 4 0 0) 35.975 0.3813 4.7916
72.103 1.3089 1.0 (-2 3 2) 36.052 0.3820 4.8004
72.449 1.3035 <1 ( 0 4 0) 36.225 0.3836 4.8203
72.642 1.3005 <1 ( 3 1 2) 36.321 0.3845 4.8314
73.580 1.2862 <1 (-3 1 3) 36.790 0.3887 4.8850
74.682 1.2700 2.0 ( 0 0 4) 37.341 0.3937 4.9476
75.046 1.2647 4.0 ( 1 4 0) 37.523 0.3954 4.9682
76.409 1.2455 1.0 (-1 1 4) 38.205 0.4015 5.0448
77.391 1.2321 <1 ( 3 3 0) 38.696 0.4058 5.0995
78.078 1.2230 <1 ( 4 0 1) 39.039 0.4088 5.1376
78.866 1.2127 1.0 ( 0 3 3) 39.433 0.4123 5.1810
附图：
PDF#00-006-0416(RDB):质标=星印(S);d=(未知);I=衍射仪
Indium Oxide
In2 O3 Light yellow
射线=CuKa1 波长=1.5405 滤波法=Ni
校准= 2θ=17.513-96.474 I/Ic(K值)=9.3
文献: Swanson et al.
Natl. Bur. Stand. (U.S.), Circ. 539, v5 p26(1955)
立方晶系-粉末衍射,Ia-3(206) Z=16
晶胞: 10.118x10.118x10.118 <90.0x90.0x90.0> P.S=cI80.00
密度(计算)=7.121 密度(测量)= 分子量=277.64 体积=1035.82 F(30)=90.4(0.0107,31/0)
文献: 出处同上
强峰线: 2.92/X 1.79/4 2.53/3 1.53/3 4.13/1 1.98/1 2.39/1 1.64/1
Additional Patterns: Validated by calculated pattern 00-044-1087.
Analysis: Spectrographic analysis: <0.1% Na, Ca; <0.001% Ag, Mg, Fe, Li, Sn, Cd, Si; <0.0001% Cu, Mn.
Color: Light yellow.
General Comments: Pattern reviewed by Holzer, J., McCarthy, G., North Dakota State University, Fargo, North Dakota, USA, JCPDS Grant-in-Aid Report (1990).
Agrees well with experimental and calculated patterns.
Additional weak reflections (indicated by brackets) were observed.
Additional Diffraction Lines: Plus 9 reflections to 0.9477.
Sample Source or Locality: Sample from Johnson Matthey Company, Ltd.
Temperature of Data Collection: Pattern taken at 299 K.
Unit Cell Data Source: Powder Diffraction.
2θ d(埃) I(f) ( h k l) θ 1/(2d) 2π/d n^2
17.513 5.0600 1.0 ( 2 0 0) 8.756 0.0988 1.2417 4
21.499 4.1300 14.0 ( 2 1 1) 10.749 0.1211 1.5214 6
30.581 2.9210 100.0 ( 2 2 2) 15.290 0.1712 2.1510 12
33.102 2.7040 2.0 ( 3 2 1) 16.551 0.1849 2.3237 14
35.466 2.5290 30.0 ( 4 0 0) 17.733 0.1977 2.4845 16
37.686 2.3850 8.0 ( 4 1 1) 18.843 0.2096 2.6345 18
39.819 2.2620 2.0 ( 4 2 0) 19.910 0.2210 2.7777 20
41.846 2.1570 6.0 ( 3 3 2) 20.923 0.2318 2.9129 22
43.782 2.0660 2.0 ( 4 2 2) 21.891 0.2420 3.0412 24
45.692 1.9840 10.0 ( 4 3 1) 22.846 0.2520 3.1669 26
49.269 1.8480 4.0 ( 5 2 1) 24.634 0.2706 3.4000 30
51.038 1.7880 35.0 ( 4 4 0) 25.519 0.2796 3.5141 32
52.715 1.7350 4.0 ( 4 3 3) 26.358 0.2882 3.6214 34
54.372 1.6860 2.0 ( 6 0 0) 27.186 0.2966 3.7267 36
55.991 1.6410 6.0 ( 6 1 1) 27.996 0.3047 3.8289 38
57.558 1.6000 2.0 ( 6 2 0) 28.779 0.3125 3.9270 40
59.137 1.5610 4.0 ( 5 4 1) 29.568 0.3203 4.0251 42
60.678 1.5250 25.0 ( 6 2 2) 30.339 0.3279 4.1201 44
62.167 1.4920 6.0 ( 6 3 1) 31.083 0.3351 4.2113 46
63.687 1.4600 6.0 ( 4 4 4) 31.843 0.3425 4.3036 48
65.135 1.4310 2.0 ( 5 4 3) 32.567 0.3494 4.3908 50
66.602 1.4030 2.0 ( 6 4 0) 33.301 0.3564 4.4784 52
68.029 1.3770 4.0 ( 7 2 1) 34.014 0.3631 4.5630 54
69.465 1.3520 2.0 ( 6 4 2) 34.732 0.3698 4.6473 56
73.661 1.2850 4.0 ( 6 5 1) 36.831 0.3891 4.8896 62
75.024 1.2650 4.0 ( 8 0 0) 37.512 0.3953 4.9669 64
76.372 1.2460 4.0 ( 7 4 1) 38.186 0.4013 5.0427 66
77.774 1.2270 2.0 ( 8 2 0) 38.887 0.4075 5.1208 68
79.157 1.2090 4.0 ( 6 5 3) 39.578 0.4136 5.1970 70
80.515 1.1920 2.0 ( 8 2 2) 40.257 0.4195 5.2711 72
81.824 1.1762 4.0 ( 8 3 1) 40.912 0.4251 5.3419 74
83.166 1.1606 6.0 ( 6 6 2) 41.583 0.4308 5.4137 76
84.504 1.1456 <1 ( 7 5 2) 42.252 0.4365 5.4846 78
85.836 1.1312 4.0 ( 8 4 0) 42.918 0.4420 5.5544 80
87.169 1.1173 2.0 ( 8 3 3) 43.585 0.4475 5.6235 82
88.490 1.1040 2.0 ( 8 4 2) 44.245 0.4529 5.6913 84
89.818 1.0911 2.0 ( 7 6 1) 44.909 0.4583 5.7586 86
91.149 1.0786 <1 ( 6 6 4) 45.575 0.4636 5.8253 88
92.484 1.0665 2.0 ( 8 5 1) 46.242 0.4688 5.8914 90
95.142 1.0436 2.0 ( 9 3 2) 47.571 0.4791 6.0207 94
96.474 1.0327 4.0 ( 8 4 4) 48.237 0.4842 6.0842 96
附图：
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