科研小记 | XRD标准卡片 PDF#00-049-0207

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PDF#00-049-0207(RDB):质标=星印(S);d=衍射仪;I=衍射仪

Lithium Titanium Oxide

Li4 Ti5 O12

射线=CuKa1 波长=1.5405 滤波法=

校准=外部(Si) 2θ=18.331-114.201 I/Ic(K值)=

文献: Tsubone, D., Hashimoto, T., Igarashi, K., Shimizu, T.

J. Ceram. Soc. Jpn. Inter. Ed., v102 p179(1994)

立方晶系-粉末衍射,Fd-3m(227) Z=

晶胞: 8.3588x8.3588x8.3588 <90.0x90.0x90.0> P.S=cF?

密度(计算)= 密度(测量)= 分子量=459.26 体积=584.03 F(19)=56.2(0.0130,26/0)

文献: 出处同上

强峰线: 4.84/X 2.09/6 2.52/5 1.48/3 1.61/2 1.41/1 1.21/1 1.92/1

Sample Preparation: Prepared from ''Li3 C O3'' and ''Li2 Ti3 O7'' at 930 C for 30 hours, followed by cooling in air.

Temperature of Data Collection: Pattern taken at 298 K.

Unit Cell Data Source: Powder Diffraction.

    2θ   d(埃)   I(f)  ( h k l)      θ  1/(2d)   2π/d  n^2  

 18.331  4.8358  100.0  ( 1 1 1)   9.166  0.1034  1.2993    3

 30.182  2.9587    1.0  ( 2 2 0)  15.091  0.1690  2.1237    8

 35.572  2.5218   45.0  ( 3 1 1)  17.786  0.1983  2.4916   11

 37.213  2.4142    2.0  ( 2 2 2)  18.606  0.2071  2.6026   12

 43.243  2.0905   62.0  ( 4 0 0)  21.621  0.2392  3.0056   16

 47.353  1.9182    6.0  ( 3 3 1)  23.676  0.2607  3.2755   19

 57.214  1.6088   20.0  ( 3 3 3)  28.607  0.3108  3.9055   27

 62.834  1.4777   33.0  ( 4 4 0)  31.417  0.3384  4.2519   32

 66.074  1.4129   11.0  ( 5 3 1)  33.037  0.3539  4.4470   35

 74.345  1.2749    4.0  ( 5 3 3)  37.173  0.3922  4.9285   43

 75.365  1.2601    2.0  ( 6 2 2)  37.682  0.3968  4.9861   44

 79.346  1.2066    7.0  ( 4 4 4)  39.673  0.4144  5.2074   48

 82.317  1.1704    5.0  ( 5 5 1)  41.158  0.4272  5.3684   51

 90.116  1.0883    4.0  ( 7 3 1)  45.058  0.4594  5.7736   59

 95.008  1.0447    3.0  ( 8 0 0)  47.504  0.4786  6.0142   64

105.909  0.9651    3.0  ( 7 5 1)  52.955  0.5181  6.5105   75

106.909  0.9588    1.0  ( 6 6 2)  53.455  0.5215  6.5531   76

111.039  0.9345    5.0  ( 8 4 0)  55.520  0.5351  6.7239   80

114.201  0.9174    2.0  ( 7 5 3)  57.100  0.5450  6.8487   83  

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