夜雨聆风PDF#00-048-1548(RDB):质标=星印(S);d=衍射仪;I=衍射仪
Tenorite, syn(Copper Oxide)
Cu O
射线=CuKa1 波长=1.540598 滤波法=Ge
校准=外部(BaF2) 2θ=32.509-120.508 I/Ic(K值)=
文献: Langford, J., Louer, D.
J. Appl. Crystallogr., v24 p149(1991)
单斜晶系-粉末衍射,C2/c(15) Z=4
晶胞: 4.6883x3.4229x5.1319 <90.0x99.506x90.0> P.S=mC8.00
密度(计算)=6.505 密度(测量)= 分子量=79.55 体积=81.22 F(30)=65.4(0.0148,31/0)
文献: 出处同上
强峰线: 2.52/X 2.32/X 2.53/4 1.87/3 2.31/2 1.51/2 1.41/2 1.38/1
Additional Patterns: To replace 00-005-0661.
Sample Preparation: ''Cu2 ( O H )3 N O3'' was thermally decomposed to form ''Cu O''.
This was annealed at 1000 C in air for 5 hours.
Unit Cell Data Source: Powder Diffraction.
2θ d(埃) I(f) ( h k l) θ 1/(2d) 2π/d n^2
32.509 2.7520 13.0 ( 1 1 0) 16.254 0.1817 2.2831
35.418 2.5324 37.0 ( 0 0 2) 17.709 0.1974 2.4812
35.544 2.5237 100.0 ( 1 1-1) 17.772 0.1981 2.4897
38.709 2.3243 99.0 ( 1 1 1) 19.354 0.2151 2.7033
38.903 2.3132 21.0 ( 2 0 0) 19.451 0.2162 2.7163
46.260 1.9610 3.0 ( 1 1-2) 23.130 0.2550 3.2042
48.717 1.8676 30.0 ( 2 0-2) 24.358 0.2677 3.3642
51.344 1.7781 1.0 ( 1 1 2) 25.672 0.2812 3.5337
53.487 1.7118 7.0 ( 0 2 0) 26.743 0.2921 3.6705
56.743 1.6211 <1 ( 0 2 1) 28.371 0.3084 3.8760
58.265 1.5823 10.0 ( 2 0 2) 29.132 0.3160 3.9710
61.525 1.5060 20.0 ( 1 1-3) 30.763 0.3320 4.1721
65.813 1.4179 10.0 ( 0 2 2) 32.906 0.3526 4.4314
66.221 1.4101 15.0 ( 3 1-1) 33.111 0.3546 4.4558
66.448 1.4059 <1 ( 3 1 0) 33.224 0.3557 4.4693
67.904 1.3792 6.0 ( 1 1 3) 33.952 0.3625 4.5556
68.124 1.3753 14.0 ( 2 2 0) 34.062 0.3636 4.5686
68.907 1.3616 <1 ( 2 2-1) 34.453 0.3672 4.6146
71.683 1.3155 <1 ( 3 1-2) 35.841 0.3801 4.7762
72.373 1.3047 5.0 ( 3 1 1) 36.186 0.3832 4.8159
72.944 1.2959 <1 ( 2 2 1) 36.472 0.3858 4.8487
74.978 1.2657 6.0 ( 0 0 4) 37.489 0.3950 4.9643
75.245 1.2618 5.0 ( 2 2-2) 37.622 0.3962 4.9794
79.733 1.2017 <1 ( 0 2 3) 39.866 0.4161 5.2285
80.157 1.1964 2.0 ( 2 0-4) 40.078 0.4179 5.2517
80.240 1.1954 <1 ( 1 1-4) 40.120 0.4183 5.2562
82.361 1.1699 4.0 ( 3 1-3) 41.181 0.4274 5.3707
83.064 1.1618 2.0 ( 2 2 2) 41.532 0.4304 5.4083
83.568 1.1560 2.0 ( 3 1 2) 41.784 0.4325 5.4351
83.568 1.1560 2.0 ( 4 0 0) 41.784 0.4325 5.4351
86.532 1.1239 1.0 ( 4 0-2) 43.266 0.4449 5.5906
86.774 1.1214 <1 ( 2 2-3) 43.387 0.4459 5.6031
87.967 1.1092 <1 ( 1 1 4) 43.984 0.4508 5.6646
88.053 1.1084 <1 ( 1 3 0) 44.027 0.4511 5.6690
89.789 1.0914 3.0 ( 1 3-1) 44.895 0.4581 5.7572
91.728 1.0733 1.0 ( 1 3 1) 45.864 0.4659 5.8541
95.565 1.0401 <1 ( 2 0 4) 47.782 0.4807 6.0409
98.391 1.0176 1.0 ( 2 2 3) 49.195 0.4913 6.1743
98.391 1.0176 1.0 ( 0 2 4) 49.195 0.4913 6.1743
99.683 1.0079 2.0 ( 3 1 3) 49.842 0.4961 6.2340
101.934 0.9916 <1 ( 4 0 2) 50.967 0.5042 6.3361
103.356 0.9818 2.0 ( 1 1-5) 51.678 0.5092 6.3994
103.564 0.9804 2.0 ( 2 2-4) 51.782 0.5100 6.4086
107.048 0.9580 2.0 ( 4 2 0) 53.524 0.5219 6.5590
109.518 0.9431 <1 ( 1 3-3) 54.759 0.5301 6.6620
110.169 0.9394 3.0 ( 4 2-2) 55.085 0.5323 6.6886
111.190 0.9336 <1 ( 4 0-4) 55.595 0.5356 6.7299
113.488 0.9212 2.0 ( 1 1 5) 56.744 0.5428 6.8210
114.059 0.9182 <1 ( 3 3-1) 57.030 0.5446 6.8432
114.059 0.9182 <1 ( 4 2 1) 57.030 0.5446 6.8432
115.743 0.9096 1.0 ( 1 3 3) 57.872 0.5497 6.9077
116.837 0.9042 <1 ( 5 1-1) 58.419 0.5530 6.9488
120.220 0.8885 1.0 ( 2 2 4) 60.110 0.5628 7.0719
120.508 0.8872 3.0 ( 3 3 1) 60.254 0.5636 7.0821
120.508 0.8872 3.0 ( 3 1-5) 60.254 0.5636 7.0821
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附图：
PDF#00-035-0822(RDB):质标=星印(S);d=衍射仪;I=衍射仪
Ferdisilicite, syn (NR)(Iron Silicon)
Fe Si2 Dark gray
射线=CuKa1 波长=1.5405982 滤波法=Graph
校准=内部(W) 2θ=17.252-141.549 I/Ic(K值)=
文献:
Natl. Bur. Stand. (U.S.) Monogr. 25, v21 p73(1985)
四方晶系-粉末衍射,P4/mmm(123) Z=1
晶胞: 2.69392x2.69392x5.1361 <90.0x90.0x90.0> P.S=tP3.00
密度(计算)=4.99 密度(测量)= 分子量=112.02 体积=37.27 F(27)=58.6(0.0118,39/0)
文献:
强峰线: 1.86/X 2.39/6 1.90/5 5.14/4 1.79/1 1.35/1 1.71/1 1.27/1
Additional Patterns: To replace 00-022-1113.
Color: Dark gray.
General Comments: An orthorhombic low temperature phase, stable below 915 C was observed by Bucksch, R., Z.
Naturforsch., Teil A, 22 2124 (1967).
Sample Source or Locality: The sample was obtained from Cerac, Inc., Milwaukee, Wisconsin, USA.
It contained some FeSi.
Temperature of Data Collection: The mean temperature of data collection was 297.8 K.
Unit Cell Data Source: Powder Diffraction.
2θ d(埃) I(f) ( h k l) θ 1/(2d) 2π/d n^2
17.252 5.1359 39.0 ( 0 0 1) 8.626 0.0974 1.2234
33.229 2.6940 2.0 ( 1 0 0) 16.614 0.1856 2.3323
37.668 2.3861 59.0 ( 1 0 1) 18.834 0.2095 2.6332
47.712 1.9046 51.0 ( 1 1 0) 23.856 0.2625 3.2989
48.969 1.8586 100.0 ( 1 0 2) 24.484 0.2690 3.3806
51.124 1.7852 12.0 ( 1 1 1) 25.562 0.2801 3.5196
53.471 1.7123 11.0 ( 0 0 3) 26.735 0.2920 3.6695
60.448 1.5303 <1 ( 1 1 2) 30.224 0.3267 4.1060
64.446 1.4446 3.0 ( 1 0 3) 32.223 0.3461 4.3493
69.764 1.3469 12.0 ( 2 0 0) 34.882 0.3712 4.6648
72.467 1.3032 3.0 ( 2 0 1) 36.234 0.3837 4.8214
73.707 1.2843 6.0 ( 0 0 4) 36.853 0.3893 4.8922
74.466 1.2731 10.0 ( 1 1 3) 37.233 0.3927 4.9353
82.095 1.1730 6.0 ( 2 1 1) 41.047 0.4263 5.3565
89.834 1.0909 1.0 ( 2 1 2) 44.917 0.4583 5.7594
92.677 1.0648 6.0 ( 1 1 4) 46.338 0.4696 5.9009
93.378 1.0586 4.0 ( 2 0 3) 46.689 0.4723 5.9353
102.835 0.9854 2.0 ( 2 1 3) 51.418 0.5074 6.3763
106.746 0.9598 2.0 ( 1 0 5) 53.373 0.5209 6.5462
107.958 0.9524 2.0 ( 2 2 0) 53.979 0.5250 6.5973
111.973 0.9293 4.0 ( 2 0 4) 55.987 0.5380 6.7613
121.123 0.8845 <1 ( 3 0 1) 60.562 0.5653 7.1037
122.494 0.8786 <1 ( 2 1 4) 61.247 0.5691 7.1511
129.458 0.8518 2.0 ( 3 1 0) 64.729 0.5870 7.3762
130.668 0.8476 3.0 ( 3 0 2) 65.334 0.5899 7.4126
135.457 0.8324 3.0 ( 2 2 3) 67.728 0.6007 7.5483
141.549 0.8158 <1 ( 1 0 6) 70.775 0.6129 7.7020
附图：
PDF#00-048-0048(RDB):质标=空白(B);d=衍射仪;I=衍射仪
Strontium Aluminum Borate
Sr Al3 B O7
射线=CuKa 波长=1.5418 滤波法=Ni
校准= 2θ=14.046-77.474 I/Ic(K值)=
文献: Jagannathan, R., Rao, R., Kutty, T.
Mater. Res. Bull., v27 p459(1992)
单斜晶系-粉末衍射,P Z=
晶胞: 13.107x9.14x5.477 <90.0x106.42x90.0> P.S=mP?
密度(计算)= 密度(测量)= 分子量=291.37 体积=629.37 F(26)=0.4(0.167,401/0)
文献: 出处同上
强峰线: 2.48/X 2.63/9 2.11/8 1.54/7 2.77/7 1.39/6 1.39/6 2.01/6
Sample Preparation: $GG-''Al2 O3'', ''Sr O'' and ''H3 B O3'' (mole ratio 3:2:2) heated to 1150 C for 4 hours.
Homogenized, reheated to 1150 C for 3 hours.
Reduced in ''N2'' and ''H2'' (90:10) at 1150 C, washed with dilute ''N H4 O H''.
A small indefinite amount (0.1-5 mole%) of ''Sr O'' was replaced by ''Eu2 O3''.
Unit Cell Data Source: Powder Diffraction.
2θ d(埃) I(f) ( h k l) θ 1/(2d) 2π/d n^2
14.046 6.3000 20.0 ( 2 0 0) 7.023 0.0794 0.9973
18.902 4.6910 41.0 ( 1 1-1) 9.451 0.1066 1.3394
20.151 4.4030 48.0 ( 1 0 1) 10.076 0.1136 1.4270
24.299 3.6600 45.0 ( 2 2 0) 12.149 0.1366 1.7167
25.652 3.4700 48.0 ( 0 2 1) 12.826 0.1441 1.8107
32.256 2.7730 71.0 ( 2 3 0) 16.128 0.1803 2.2658
34.049 2.6310 89.0 ( 0 0 2) 17.024 0.1900 2.3881
35.108 2.5540 54.0 (-2 3 1) 17.554 0.1958 2.4601
36.206 2.4790 100.0 ( 3 3 0) 18.103 0.2017 2.5346
37.851 2.3750 41.0 ( 1 1 2) 18.925 0.2105 2.6456
39.402 2.2850 55.0 ( 0 4 0) 19.701 0.2188 2.7498
40.952 2.2020 50.0 ( 2 0 2) 20.476 0.2271 2.8534
42.845 2.1090 81.0 ( 3 3 1) 21.422 0.2371 2.9792
43.494 2.0790 53.0 (-5 1 2) 21.747 0.2405 3.0222
45.044 2.0110 63.0 ( 1 4 1) 22.522 0.2486 3.1244
52.650 1.7370 40.0 ( 0 5 1) 26.325 0.2879 3.6173
53.412 1.7140 38.0 (-3 4 2) 26.706 0.2917 3.6658
57.558 1.6000 51.0 ( 5 0 2) 28.779 0.3125 3.9270
58.601 1.5740 54.0 ( 8 0 0) 29.300 0.3177 3.9919
58.601 1.5740 54.0 (-5 2 3) 29.300 0.3177 3.9919
60.068 1.5390 72.0 ( 3 5 1) 30.034 0.3249 4.0826
66.602 1.4030 37.0 ( 2 3 3) 33.301 0.3564 4.4784
67.362 1.3890 64.0 ( 9 0 0) 33.681 0.3600 4.5235
67.362 1.3890 64.0 ( 0 4 3) 33.681 0.3600 4.5235
68.311 1.3720 38.0 ( 4 0 3) 34.155 0.3644 4.5796
71.653 1.3160 35.0 ( 4 2 3) 35.826 0.3799 4.7745
71.653 1.3160 35.0 ( 0 0 4) 35.826 0.3799 4.7745
76.882 1.2390 33.0 ( 3 4 3) 38.441 0.4036 5.0712
77.474 1.2310 35.0 ( 5 2 3) 38.737 0.4062 5.1041
附图：
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