夜雨聆风PDF#00-028-1192(RDB):质标=定胞(I);d=(未知);I=衍射仪
Sodium Yttrium Ytterbium Erbium Fluoride
Na ( Y0.57 Yb0.39 Er0.04 ) F4
射线=CuKa1 波长=1.54051 滤波法=Ni
校准= 2θ=17.137-138.035 I/Ic(K值)=
文献: Fujii, H., Central Research Laboratory Hitachi Limited, Tokyo, Japan.
Private Communication(1975)
六方晶系-粉末衍射 Z=
晶胞: 5.96x5.96x3.51 <90.0x90.0x120.0> P.S=h??
密度(计算)= 密度(测量)= 分子量=223.84 体积=107.98 F(30)=54.4(0.0167,33/0)
文献: Kano, T. et al.
J. Electrochem. Soc., v119 p1561(1972)
强峰线: 5.17/X 2.98/9 2.90/8 2.08/7 1.71/6 1.72/4 2.27/2 1.12/1
Unit Cell Data Source: Powder Diffraction.
2θ d(埃) I(f) ( h k l) θ 1/(2d) 2π/d n^2
17.137 5.1700 100.0 ( 1 0 0) 8.569 0.0967 1.2153
25.354 3.5100 <1 ( 0 0 1) 12.677 0.1425 1.7901
29.961 2.9800 85.0 ( 1 1 0) 14.980 0.1678 2.1085
30.807 2.9000 75.0 ( 1 0 1) 15.404 0.1724 2.1666
34.743 2.5800 12.0 ( 2 0 0) 17.371 0.1938 2.4353
39.673 2.2700 16.0 ( 1 1 1) 19.836 0.2203 2.7679
43.472 2.0800 70.0 ( 2 0 1) 21.736 0.2404 3.0208
46.510 1.9510 12.0 ( 2 1 0) 23.255 0.2563 3.2205
52.069 1.7550 6.0 ( 0 0 2) 26.035 0.2849 3.5802
53.178 1.7210 35.0 ( 3 0 0) 26.589 0.2905 3.6509
53.717 1.7050 55.0 ( 2 1 1) 26.858 0.2933 3.6852
55.259 1.6610 7.0 ( 1 0 2) 27.630 0.3010 3.7828
59.811 1.5450 <1 ( 3 0 1) 29.906 0.3236 4.0668
61.255 1.5120 8.0 ( 1 1 2) 30.627 0.3307 4.1555
62.259 1.4900 9.0 ( 2 2 0) 31.130 0.3356 4.2169
64.129 1.4510 3.0 ( 2 0 2) 32.064 0.3446 4.3302
65.084 1.4320 4.0 ( 3 1 0) 32.542 0.3492 4.3877
68.311 1.3720 <1 ( 2 2 1) 34.155 0.3644 4.5796
71.030 1.3260 11.0 ( 3 1 1) 35.515 0.3771 4.7385
72.352 1.3050 4.0 ( 2 1 2) 36.176 0.3831 4.8147
73.263 1.2910 1.0 ( 4 0 0) 36.631 0.3873 4.8669
77.624 1.2290 8.0 ( 3 0 2) 38.812 0.4068 5.1124
79.001 1.2110 3.0 ( 4 0 1) 39.500 0.4129 5.1884
81.172 1.1840 1.0 ( 3 2 0) 40.586 0.4223 5.3067
84.925 1.1410 2.0 ( 1 0 3) 42.462 0.4382 5.5067
85.387 1.1360 3.0 ( 2 2 2) 42.694 0.4401 5.5310
86.330 1.1260 9.0 ( 4 1 0) 43.165 0.4440 5.5801
86.713 1.1220 13.0 ( 3 2 1) 43.357 0.4456 5.6000
87.988 1.1090 3.0 ( 3 1 2) 43.994 0.4509 5.6656
92.540 1.0660 2.0 ( 2 0 3) 46.270 0.4690 5.8942
95.577 1.0400 1.0 ( 4 0 2) 47.788 0.4808 6.0415
96.561 1.0320 <1 ( 5 0 0) 48.280 0.4845 6.0884
100.348 1.0030 4.0 ( 2 1 3) 50.174 0.4985 6.2644
101.742 0.9930 2.0 ( 3 3 0) 50.871 0.5035 6.3275
102.026 0.9910 4.0 ( 5 0 1) 51.013 0.5045 6.3402
103.333 0.9820 2.0 ( 3 2 2) 51.667 0.5092 6.3984
108.691 0.9480 6.0 ( 4 1 2) 54.346 0.5274 6.6278
110.062 0.9400 5.0 ( 4 2 1) 55.031 0.5319 6.6842
112.394 0.9270 <1 ( 5 1 0) 56.197 0.5394 6.7780
116.470 0.9060 2.0 ( 3 1 3) 58.235 0.5519 6.9351
118.567 0.8960 4.0 ( 5 1 1) 59.283 0.5580 7.0125
119.880 0.8900 1.0 ( 5 0 2) 59.940 0.5618 7.0598
125.361 0.8670 1.0 ( 4 0 3) 62.680 0.5767 7.2470
125.876 0.8650 3.0 ( 1 0 4) 62.938 0.5780 7.2638
127.195 0.8600 <1 ( 6 0 0) 63.597 0.5814 7.3060
129.122 0.8530 <1 ( 4 2 2) 64.561 0.5862 7.3660
130.561 0.8480 <1 ( 4 3 0) 65.281 0.5896 7.4094
132.366 0.8420 <1 ( 1 1 4) 66.183 0.5938 7.4622
135.589 0.8320 3.0 ( 3 2 3) 67.795 0.6010 7.5519
137.675 0.8260 3.0 ( 5 2 0) 68.838 0.6053 7.6068
138.035 0.8250 4.0 ( 4 3 1) 69.018 0.6061 7.6160
附图：
PDF#01-077-2042(RDB):质标=定胞(I);d=计算值;I=计算值
Sodium Yttrium Fluoride
Na Y F4
射线=CuKa1 波长=1.5406 滤波法=
校准= 2θ=28.235-138.169 I/Ic(K值)=4.93
文献: Roy, D.M., Roy, R.
J. Electrochem. Soc., v111 p421(1964)
立方晶系-粉末衍射,Fm-3m(225) Z=2
晶胞: 5.47x5.47x5.47 <90.0x90.0x90.0> P.S=cF12.00
密度(计算)=3.813 密度(测量)= 分子量=187.89 体积=163.67 F(16)=999.9(0.0003,16/0)
文献: 出处同上
强峰线: 3.16/X 1.93/8 1.65/3 1.12/1 1.25/1 1.37/1 1.05/1 0.92/1
ANX: AX2.
Analysis: F4 Na1 Y1.
Formula from original source: Na Y F4.
ICSD Collection Code: 60257.
Calculated Pattern Original Remarks: Stable above 978 K (2nd ref., Tomaszewski), 964-978 K: P63/m.
Minor Warning: No e.s.d reported/abstracted on the cell dimension.
No R factors reported/abstracted.
Wyckoff Sequence: c a(FM3-M).
Unit Cell Data Source: Powder Diffraction.
2θ d(埃) I(f) ( h k l) θ 1/(2d) 2π/d n^2
28.235 3.1581 100.0 ( 1 1 1) 14.117 0.1583 1.9895 3
32.717 2.7350 4.1 ( 2 0 0) 16.358 0.1828 2.2973 4
46.944 1.9339 80.6 ( 2 2 0) 23.472 0.2585 3.2489 8
55.686 1.6493 31.8 ( 3 1 1) 27.843 0.3032 3.8097 11
58.395 1.5791 1.4 ( 2 2 2) 29.198 0.3166 3.9791 12
68.567 1.3675 8.7 ( 4 0 0) 34.283 0.3656 4.5947 16
75.734 1.2549 9.6 ( 3 3 1) 37.867 0.3984 5.0069 19
78.067 1.2231 1.9 ( 4 2 0) 39.033 0.4088 5.1370 20
87.242 1.1166 13.0 ( 4 2 2) 43.621 0.4478 5.6273 24
94.064 1.0527 6.0 ( 5 1 1) 47.032 0.4750 5.9686 27
105.615 0.9670 3.6 ( 4 4 0) 52.807 0.5171 6.4978 32
112.840 0.9246 5.9 ( 5 3 1) 56.420 0.5408 6.7956 35
115.329 0.9117 1.1 ( 6 0 0) 57.664 0.5484 6.8920 36
125.906 0.8649 5.3 ( 6 2 0) 62.953 0.5781 7.2648 40
134.866 0.8342 2.4 ( 5 3 3) 67.433 0.5994 7.5323 43
138.169 0.8246 0.7 ( 6 2 2) 69.084 0.6063 7.6194 44
附图：
PDF#00-044-0926(RDB):质标=空白(B);d=(未知);I=胶片/目测
Rubidium Antimony Oxide
Rb4 Sb2 O7
射线=CuKa1 波长=1.5406 滤波法=
校准= 2θ=16.972-49.641 I/Ic(K值)=
文献: Josien, F.-A., Duquenoy, G.
Rev. Chim. Miner., v17 p40(1980)
立方晶系-粉末衍射 Z=
晶胞: 8.995x8.995x8.995 <90.0x90.0x90.0> P.S=c??
密度(计算)= 密度(测量)= 分子量=697.37 体积=727.79 F(10)=6.1(0.078,21/0)
文献: 出处同上
强峰线: 3.18/X 2.25/2 1.84/2 3.00/2 2.83/1 2.72/1 5.22/1
Sample Preparation: Prepared by solid-state reaction between ''Rb3 Sb O4'' and ''Sb2 O3'' in 4:1 ratio.
Unit Cell Data Source: Powder Diffraction.
2θ d(埃) I(f) ( h k l) θ 1/(2d) 2π/d n^2
16.972 5.2200 5.0 ( 1 1 1) 8.486 0.0958 1.2037 3
22.150 4.0100 2.0 ( 0 1 2) 11.075 0.1247 1.5669 5
28.019 3.1820 100.0 ( 0 2 2) 14.009 0.1571 1.9746 8
29.807 2.9950 15.0 ( 0 0 3) 14.904 0.1669 2.0979 9
31.589 2.8300 10.0 ( 0 1 3) 15.795 0.1767 2.2202 10
32.964 2.7150 10.0 ( 1 1 3) 16.482 0.1842 2.3142 11
37.523 2.3950 2.0 ( 1 2 3) 18.761 0.2088 2.6235 14
40.134 2.2450 20.0 ( 0 0 4) 20.067 0.2227 2.7987 16
45.163 2.0060 2.0 ( 0 2 4) 22.581 0.2493 3.1322 20
49.641 1.8350 20.0 ( 2 2 4) 24.821 0.2725 3.4241 24
附图：
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